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In situ TiC reinforced Ti6Al4V matrix composites manufactured via selective laser melting

İdris Tuğrul Gülenç (Department of Materials Science and Engineering, The University of Sheffield, Sheffield, UK)
Mingwen Bai (Centre for Manufacturing and Materials, Coventry University, Coventry, UK and Department of Materials Science and Engineering, The University of Sheffield, Sheffield, UK, and)
Ria L. Mitchell (Department of Materials Science and Engineering, The University of Sheffield, Sheffield, UK)
Iain Todd (Department of Materials Science and Engineering, The University of Sheffield, Sheffield, UK)
Beverley J. Inkson (Department of Materials Science and Engineering, The University of Sheffield, Sheffield, UK)

Rapid Prototyping Journal

ISSN: 1355-2546

Article publication date: 20 December 2023

Issue publication date: 7 February 2024

153

Abstract

Purpose

Current methods for the preparation of composite powder feedstock for selective laser melting (SLM) rely on costly nanoparticles or yield inconsistent powder morphology. This study aims to develop a cost-effective Ti6Al4V-carbon feedstock, which preserves the parent Ti6Al4V particle’s flowability, and produces in situ TiC-reinforced Ti6Al4V composites with superior traits.

Design/methodology/approach

Ti6Al4V particles were directly mixed with graphite flakes in a planetary ball mill. This composite powder feedstock was used to manufacture in situ TiC-Ti6Al4V composites using various energy densities. Relative porosity, microstructure and hardness of the composites were evaluated for different SLM processing parameters.

Findings

Homogeneously carbon-coated Ti6Al4V particles were produced by direct mixing. After SLM processing, in situ grown 100–500 nm size TiC nanoparticles were distributed within the α-martensite Ti6Al4V matrix. The formation of TiC particles refines the Ti6Al4V β grain size. Relative density varied between 96.4% and 99.5% depending on the processing parameters. Hatch distance, exposure time and point distance were all effective on relative porosity change, whereas only exposure time and point distance were effective on hardness change.

Originality/value

This work introduces a novel, cost-effective powder feedstock preparation method for SLM manufacture of Ti6Al4V-TiC composites. The in situ SLM composites achieved in this study have high relative density values, well-dispersed TiC nanoparticles and increased hardness. In addition, the feedstock preparation method can be readily adapted for various matrix and reinforcement materials in future studies.

Keywords

Acknowledgements

Since submission of this article, the following author has updated their affiliation: İdris Tuğrul Gülenç is at the Department of Metallurgical and Materials Engineering, Ankara Yıldırım Beyazıt University, Ankara, Türkiye.

Citation

Gülenç, İ.T., Bai, M., Mitchell, R.L., Todd, I. and Inkson, B.J. (2024), "In situ TiC reinforced Ti6Al4V matrix composites manufactured via selective laser melting", Rapid Prototyping Journal, Vol. 30 No. 2, pp. 378-392. https://doi.org/10.1108/RPJ-01-2023-0027

Publisher

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Emerald Publishing Limited

Copyright © 2023, Emerald Publishing Limited

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